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Lecturer(s)
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Čech Bohumil, prof. Ing. Ph.D.
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Nemec M., Ing. Ph.D.
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Michalík Michal, Ing. Ph.D.
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Course content
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1. General aspects of the use of methods of material analysis in electrical engineering 2. Relation of structure and physicochemical properties of substances 3. Overview of methods and measured parameters for determination of properties of substances 4. Basic concepts and classification of structural analyses 5. Differential thermal analysis and differential scanning calorimetry (basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice) 6. Thermogravimetry and Derivative Thermogravimetry (basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice) 7. Dilatometry and thermomechanical analysis (basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice) 8. Rheology and dynamic mechanical analysis (basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice, TTS diagrams) 9. Utilization of thermal analyses in the study of kinetics of chemical reactions 10. Separation techniques - basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice 11. Infrared spectroscopy - basic principles, overview of measuring techniques, design of IR spectrometers 12. Infrared spectroscopy - qualitative and quantitative methods of analysis, examples of the use of IR spectroscopy techniques in practice 13. Broadband dielectric spectroscopy and other special techniques of material analysis and their use
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Learning activities and teaching methods
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Laboratory work, Lecture
- Contact hours
- 26 hours per semester
- Practical training (number of hours)
- 26 hours per semester
- Preparation for laboratory testing; outcome analysis (1-8)
- 8 hours per semester
- Preparation for an examination (30-60)
- 45 hours per semester
- Graduate study programme term essay (40-50)
- 45 hours per semester
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| prerequisite |
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| Knowledge |
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| no particular prerequisites are specified |
| Skills |
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| no particular prerequisites are specified |
| learning outcomes |
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| Knowledge |
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| clarify the basic relationships between the structure and the physicochemical properties of the substances |
| known the basic classification of methods and corresponding material properties used for physicochemical analysis of materials |
| explain the basic principles of methods of material analysis of materials used in electrical engineering |
| describe the design of the measuring instruments used for the material analysis |
| evaluate on a particular example the advantages and disadvantages of applying a particular method |
| Skills |
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| uses practically differential scanning calorimetry, thermogravimetry, thermomechanical analysis, dynamic mechanical analysis, Fourier transform infrared spectroscopy and broadband dielectric spectroscopy |
| measures the material properties corresponding to the method |
| finds appropriate professional literature |
| evaluate the measured data on the basis of its own experience and with the help of specialized literature |
| teaching methods |
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| Knowledge |
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| Lecture supplemented with a discussion |
| Multimedia supported teaching |
| Self-study of literature |
| Skills |
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| Laboratory work |
| assessment methods |
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| Knowledge |
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| Combined exam |
| Skills |
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| Skills demonstration during practicum |
| Individual presentation at a seminar |
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Recommended literature
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Askeland, Donald R.; Fulay, Pradeep P.,; Wright, Wendelin J. The science and engineering of materials. 6th ed. Stamford : Cengage Learning, 2011. ISBN 978-0-495-29602-7.
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Crompton, T. R. Physical testing of plastics. Shrewsbury : Smithers Rapra Technology, 2012. ISBN 978-1-84735-485-3.
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Griffiths, Peter R.; De Haseth, James A. Fourier transform infrared spectrometry. 2nd ed. Hoboken : Wiley-Interscience, 2007. ISBN 978-0-471-19404-0.
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Mentlík, Václav. Diagnostika elektrických zařízení. Praha : BEN - technická literatura, 2008. ISBN 978-80-7300-232-9.
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Wunderlich, Bernhard. Thermal analysis of polymeric materials. Berlin : Springer, 2005. ISBN 978-3-540-23629-0.
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