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Lecturer(s)
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Nuruyev Jiří, doc. Mgr. CSc.
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Pelikán Jakub, Mgr. Ph.D.
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Course content
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1st practise Safety in the chemical laboratory. Practical introduction to semimicrotechnics, preparing of basic tools for working with small quanta. Determination of Koffler method, purity verification of compound by thin-flim chromatography. 2nd practise to 6th practise Basic synthesis of organic compounds (esterification, nitration, oxidation, reduction, diazotation, copulation, etc.). Isolation of product from the reaction mixture after synthesis. Isolation of organic compounds from natural material. Identification upcoming preparations. Practises are chosen in ways to use the maximum of chemicals at current utilisation of all isolation processes (distillation, steam distillation, distillation under reduced pressure, crystallization) and methods of purity verification. Note: All of students begin in 2nd pracits with the preparation of ethylacetate, after comes the preparation od adipic acid and benzol acid (3rd practise). 4th, 5th and 6th practises are individual according to the students ability and skills (knack).
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Learning activities and teaching methods
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Laboratory work
- Contact hours
- 52 hours per semester
- Preparation for formative assessments (2-20)
- 7 hours per semester
- Preparation for laboratory testing; outcome analysis (1-8)
- 8 hours per semester
- Practical training (number of hours)
- 52 hours per semester
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| prerequisite |
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| Knowledge |
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| use knowledge of safe work in the lab |
| take advantage of the experience gained from laboratory work and inorganic chemistry exercises |
| use the knowledge of inorganic and organic chemistry |
| Skills |
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| to control the principles of safe working with chemicals |
| to build simple and more complicated appliances |
| record procedures and work results |
| learning outcomes |
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| Knowledge |
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| apply theoretical knowledge in solving laboratory procedures |
| to anticipate the course of chemical transformations |
| to propose methods for product isolation |
| Skills |
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| perform the reactions as instructed |
| to insulate the prepared products |
| to propose innovative procedures |
| teaching methods |
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| Knowledge |
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| Laboratory work |
| assessment methods |
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| Skills demonstration during practicum |
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Recommended literature
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Klinotová, E.; Klinot, J.; Máca, B.; Trnka, T.; Všetečka, V. Základní cvičení z organické chemie. Praha: Univerzita Karlova, 1980.
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MAYO D. W., PIKE R. M., TRUMPER P. K. Microscale Techniques for the Organic Laboratory. John Wiley & sons, inc., New York, 2001. ISBN 0-471-24909-2.
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MOHRIG J. R., HAMMOND C. N., SCHATZ P. F., MORRILL T. C. Modern Projects and Experiments in Organic Chemistry. W. H. Freeman and Company, New York, 2003. ISBN 0-7167-9779-8.
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Richtr, Václav. Semimikrotechnika v organické chemii. 1. vyd. Plzeň : Pedagogická fakulta Západočeské univerzity, 1993. ISBN 80-7043-066-4.
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Trnka, Tomáš. Praktikum z organické chemie : Určeno pro posl. fak. přírodověd.. 1. vyd. Praha : SPN, 1986.
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VESELÝ, J., MACHARA, A. Příručka laboratorní organické chemie. Vydavatelství ČVUT, 2020. ISBN 978-80-7444-076-2.
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