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Lecturer(s)
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Šabata Pavel, PaedDr. CSc.
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Bunda Jiří, Ing. Ph.D.
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Course content
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1st exercise Basic rules for the preparation of inorganic compounds in the laboratory. Basic methods of preparation of inorganic compounds. 2nd exercise Neutralization reaction, substitution reaction. Dissolution of metals and oxides in acids. 3rd exercise Clotting reaction. 4th exercise Preparation, drying and storage of gases. The use of gases in the preparation. Annealing in the gas stream. Redox reactions, oxidation and reduction by the gas. 5th exercise Insulation from melts. Preparation of complex compounds. 6th exercise Working at high temperatures, strong exothermic reaction. Working with toxic chemicals. Works are chosen according to approved method, in part becaouse consecutive preparative schemes. In the preparations are done simple analytical verification.
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Learning activities and teaching methods
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Laboratory work, Skills demonstration, Individual study
- Practical training (number of hours)
- 52 hours per semester
- Preparation for formative assessments (2-20)
- 10 hours per semester
- Contact hours
- 52 hours per semester
- Preparation for laboratory testing; outcome analysis (1-8)
- 8 hours per semester
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| prerequisite |
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| Knowledge |
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| to describe the properties of the elements and their compounds |
| to explain the behavior of elements and their compounds in chemical processes |
| Skills |
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| to apply basic knowledge about the course of chemical reactions on specific examples of inorganic chemistry |
| perform basic chemical calculations and apply them to solve practical problems in the laboratory |
| to use chemical terminology in describing substances and explaining chemical processes |
| learning outcomes |
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| Knowledge |
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| to describe basic laboratory methods of preparative inorganic chemistry |
| Skills |
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| to prepare selected inorganic compounds by neutralization, dissolution of metals and oxides in acids, precipitation reactions |
| to prepare selected inorganic compounds with gas preparations, redox preparations and melt insulation |
| to apply theoretical knowledge to model situations in the preparation of inorganic compounds |
| teaching methods |
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| Knowledge |
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| Laboratory work |
| Skills demonstration |
| Individual study |
| assessment methods |
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| Test |
| Skills demonstration during practicum |
| Individual presentation at a seminar |
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Recommended literature
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Klikorka, Jiří. Úvod do preparativní anorganické chemie. Praha : SNTL - nakladatelství technické literatury, 1974.
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Podlahová, Jana. Cvičení z preparativní anorganické chemie. Praha : Státní pedagogické nakladatelství, 1974.
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Sýkorová, D. Návody pro laboratoře z anorganické chemie. Praha: VŠCHT, 2001. ISBN 80-7080-425-1.
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